Heat treatment effect on microstructure evolution of two steels manufactured by laser powder bed fusion

Additive manufacturing technology represents a valid alternative for the production of ferromagnetic components in Si steels (FeSi) with high Si content. In this work the effect of heat treatments on microstructural evolution of two steels with standard (3.0 wt.% - FeSi3) and high (6.5 wt.% - FeSi6.5) Si content manufactured by Laser Powder Bed Fusion (L-PBF) was investigated. Four different temperatures ranging from 900 °C up to 1150 °C (soaking time of 1 hour) were tested for each steel. In as-built condition, all the grains of FeSi3 are columnar with the [100] direction parallel to the building direction (BD) whereas in the case of FeSi6.5 there is a mix of columnar and equiaxed grains. The average grain size of FeSi6.5 (11.3 ± 0.6 μm) is about one order of magnitude lower than that of FeSi3 (103.1 ± 5.2 μm). EBSD analysis revealed that there is a prevalence of low-angle boundaries (LABs) in FeSi3 and of high-angle boundaries (HABs) in FeSi6.5. The different initial microstructure affects the response to heat treatments of the two alloys: grain size and shape of FeSi3 do not remarkably change, on the contrary significant grain growth takes place in FeSi6.5 without a weakening of the [100] texture. No brittle ordered phases were detected in as-built and heat-treated samples of both materials. The results indicate that heat treatments at high temperature can be exploited to improve the magnetic characteristics of printed FeSi6.5 and reach similar properties of commercial steels.